EPA Method 7741A

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EPA Method 7741A:

Samples are prepared according to the nitric/sulfuric acid digestion procedure described in this method. Next, the selenium in the digestate is reduced to Se(IV) with tin chloride. The Se(IV) is then converted to a volatile hydride with hydrogen produced from a zinc/HCl or sodium borohydrate/HCl reaction.

Method 7741 is an atomic absorption procedure that is approved for determining the concentration of selenium in wastes, mobility-procedure extracts, soils, and ground water, provided that the sample matrix does not contain high concentrations of chromium, copper, mercury, silver, cobalt, or molybdenum. All samples must be subjected to an appropriate dissolution step prior to analysis. Spiked samples and relevant standard reference materials are employed to determine applicability of the method to a given waste.

Report Number:
SW-846 Ch 3.3