EPA Method 8323

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EPA Method 8323:
DETERMINATION OF ORGANOTINS BY MICRO-LIQUID CHROMATOGRAPHY- ELECTROSPRAY ION TRAP MASS SPECTROMETRY

Summary:
This method provides reversed-phase micro-liquid chromatographic (?LC) and electrospray (ES) mass spectrometric (MS) conditions for the detection of the target analytes.

Scope:
This method covers the use of solid-phase extraction (SPE) discs, solvent extractions (for biological tissues), and micro-liquid chromatography (?LC) coupled with electrospray ion trap mass spectrometry (ES-ITMS) [this technique would also be applicable to ES-quadrupole mass spectrometry (ES-MS)] for the determination of organotins (as the cation) in waters and biological tissues.

Report Number:
SW-846